Development of Ultra-Carbon Steel Prepared by Mechanical Alloying and Subsequent Hot Pressing  

Oleh:

Rochman, Nurul Taufiqu ; Sueyoshi, H.

Jenis: Article from Journal - ilmiah nasional - terakreditasi DIKTI
Dalam koleksi: IPTEK: The Journal for Technology and Science vol. 19 no. 1 (Feb. 2008), page 7-11.
Topik: Mechanical Alloying; Ultra-Carbon Steel; Fine Grain Fertile; Fine Cementite; Hhot Pressing; Heat Treatment

Ketersediaan

Perpustakaan Pusat (Semanggi) Nomor Panggil: MM48.4 Non-tandon: 1 (dapat dipinjam: 0) Tandon: tidak ada

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Isi artikel

It is known that the most effective way to improve mechanical properties of steels is by microstructureal refinement. Iron and graphite powders mixture with hypoeutectoid composition were mechanically alloyed (MAed) and subsequently hot pressed (HPed) to provide steels with fine structure. Mechanical Alloying (MA) was carried out using a planetary ball mill for 100, 200 and 300 h, while HP at 41 MPa at various temperatures: 610 celcius degree (below), 730 celcius degree (near) and 800 celcius degree (above the eutectoid transformation point A1). The mechanically alloyed (MAed) powders were characterized by X-ray diffraction (XRD), differential thermal analysis (DTA) and scanning electron microscopy (SEM). While, the HPed compacts were characterized by SEM, Vickers hardness and tensile test. During MA, refinement or crystallite, formations of super-saturated iron solid solution and Fe/C amorphous phase occured first. With further MA time, these phases might begin to transform to more stable phases such as carbides. In the case of HP at 610 celcius degree (below A1), very fine cementites were precipitated in fine ferrite grain with sub-micron meter in the size. However, the mechanical properties cannot be attained because of low sinterability. At 730 celcius degree (near A1), the strength reaches the maximum value. With further temperature increase (at 800 celcius degree), the sintering progressed well and the coarseing occured, resulting the decrease in strength. However, the fracture strain increased significantly. The steels obtained in the present study had mechanical properties comparable to those of standard (JIS) steels through the well established heat treatment such as normalizing and thermal refining.

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