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ArtikelAtomic-Scale Chemical Imaging of Composition and Bonding by Aberration-Corrected Microscopy  
Oleh: Muller, D.A. ; Kourkoutis, L. Fitting ; Murfitt, M. ; Song, J.H. ; Hwang, H.Y. ; Silcox, J. ; Dellby, N. ; Krivanek, O.L.
Jenis: Article from Bulletin/Magazine
Dalam koleksi: SCIENCE (keterangan: ada di Proquest) vol. 319 no. 5866 (Feb. 2008), page 1073.
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  • Perpustakaan FK
    • Nomor Panggil: S01.K.2008.02
    • Non-tandon: 1 (dapat dipinjam: 0)
    • Tandon: tidak ada
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Isi artikelUsing a fifth-order aberration-corrected scanning transmission electron microscope, which provides a factor of 100 increase in signal over an uncorrected instrument, we demonstrated two-dimensional elemental and valence-sensitive imaging at atomic resolution by means of electron energy-loss spectroscopy, with acquisition times of well under a minute (for a 4096-pixel image). Applying this method to the study of a La0.7Sr0.3MnO3/SrTiO3 multilayer, we found an asymmetry between the chemical intermixing on the manganese-titanium and lanthanum-strontium sublattices. The measured changes in the titanium bonding as the local environment changed allowed us to distinguish chemical interdiffusion from imaging artifacts.
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